HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Chloropyridin-3-yl)ethan-1-one → HCID 67509657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Chloropyridin-3-yl)ethan-1-one | HCID 2779698 | — |
| Reactant | 2,2,2-Trifluoroethanethiol | HCID 4133924 | — |
| Product | HCID 67509657 | HCID 67509657 | 64% |
Reaction Steps
The title compound is prepared in 64% yield (0.39 g, an orange solid) from 1-(6-chloropyridin-3-yl)ethanone (0.40 g, 2.54 mmol) and 2,2,2-trifluoroethanethiol instead of 2,2,2-trifluoroethanol by the similar manner in Step-1 of Amine-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302991B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-97cf426ceb5e4a5b80bfd25a4ae1908b |
| Source note | uspto-grants-2016_04 |