HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylsulfinamide, (R)-(+)- → HCID 67510091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| Reactant | 1-[3-Chloro-5-(trifluoromethoxy)phenyl]ethan-1-one | HCID 17750741 | — |
| Product | HCID 67510091 | HCID 67510091 | 48% |
Reaction Steps
The title compound is prepared in 48% yield (416 mg, a white solid) from 1-(3-chloro-5-(trifluoromethoxy)phenyl)ethanone (600 mg, 2.51 mmol, Step-2) and (R)-2-methylpropane-2-sulfinamide (457 mg, 3.77 mmol) by the similar manner in Step-4 of Amine-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302991B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-d6256ec4319247ee8cc224e4104e33d7 |
| Source note | uspto-grants-2016_04 |