HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyryl chloride → HCID 67509689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyryl chloride | HCID 8855 | — |
| Reactant | methyl 2-aminoisonicotinate hydrochloride（WS204501） | HCID 67509862 | — |
| Product | HCID 67509689 | HCID 67509689 | 82% |
Reaction Steps
The title compound is prepared in 82% yield (1.94 g, a white solid) from methyl 2-aminoisonicotinate hydrochloride (2.00 g, 10.6 mmol) and butyryl chloride by the similar manner in Step-1 of Carboxylic acid-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302991B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-a0be20038da74f918955558978707c20 |
| Source note | uspto-grants-2016_04 |