HRID623967

反应详情

EQUATION

反应方程式

HRID 623967 的结构方程式

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

The title compound was prepared using 6-bromo-2-chloro-3-phenoxy-4-(trifluoromethyl)quinoline (Intermediate 8, step b) in place of 6-bromo-2,4-dichloro-3-phenoxyquinoline (Intermediate 5, step c) according to the procedure described in Intermediate 5, step d except the reaction mixture was heated at 100° C. under reflux condenser for 2.5 hours.

WORKUP

后处理

  1. temperatureunder reflux condenser for 2.5 hours