HCID 68283595, compound → HCID 67127466, compound

Participants

Reaction Steps

To a solution of 1-(3-methoxyphenethyl)-4-nitro-1H-pyrazole (2.03 mmol) in EtOAc (2 mL, degassed) and EtOH (6 mL, degassed), PtO2 (45 mg, 0.20 mmol) was added and the reaction mixture was stirred at rt under a H2-atmosphere for 3 h. The mixture was diluted with EtOH, filtered over celite and the filter cake was rinsed with EtOH. The filtrate was concentrated to obtain the title compound as red oil. LC-MS conditions A: tR=0.52 min, [M+H]+=218.42.

Provenance & Evidence