HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoroindole → 3-(2-bromoethyl)-5-fluoro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoroindole | HCID 67861 | — |
| Reactant | 3-(2-bromoethyl)-5-methoxy-1H-indole | HCID 11107868 | — |
| Product | 3-(2-bromoethyl)-5-fluoro-1H-indole | HCID 11207226 | — |
Reaction Steps
The title compound was synthesized according to above mentioned procedure for 3-(2-bromoethyl)-5-methoxy-1H-indole, starting with 5-fluoroindole yielding a brown oil which was stored in the freezer. LC-MS conditions B: tR=0.82 min, [M(81Br)+MeCN+H]+=244.07.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303023B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-8f8a52b730eb475cb6355e44fb91ae6c |
| Source note | uspto-grants-2016_04 |