HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-furaldehyde → HCID 86722896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-furaldehyde | HCID 2769630 | — |
| Reactant | HCID 86722897 | HCID 86722897 | — |
| Product | HCID 86722896 | HCID 86722896 | — |
Reaction Steps
The title compound was prepared from (S)-6-(2-hydroxypropyl)-1,3-dimethyl-5-m-tolyl-1H-pyrrolo[3,4-d]pyrimidine-2,4(3H,6H)-dione and 5-chlorofuran-2-carbaldehyde by an analogous method to Example 12. Purification was carried out by chromatography on silica eluting with 0-55% EtOAc in iso-hexane;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303035B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-27665d7bd57f42b78ec2446670726b20 |
| Source note | uspto-grants-2016_04 |