HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → 1-isopropyl-3-methyl-1H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | N'-isopropylacetohydrazonamide | HCID 74037752 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-isopropyl-3-methyl-1H-1,2,4-triazole | HCID 20744898 | — |
Reaction Steps
N′-isopropylacetohydrazonamide 6 was treated with triethylorthoformate in ethanol, followed by triethylamine and tetrahydrofuran to give 7 (CAS Reg. No. 1401305-30-3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303043B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-1addbd14bf194fe1a751b33466e25dd5 |
| Source note | uspto-grants-2016_04 |