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HRID624864

反应详情

EQUATION

反应方程式

HRID 624864 的结构方程式

REACTANTS

反应物

4
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CNC(C)(C)CO
HCID422780

2-methyl-2-(methylamino)propan-1-ol

C5H13NO

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：CC(Oc1nc(C(=O)O)ccc1C1CC1)C(F)(F)F
HCID71087435

未命名化合物

PRODUCTS

生成物

1
结构：CC(Oc1nc(C(=O)N(C)C(C)(C)C)ccc1C1CC1)C(F)(F)F
HCID90203497

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in Example 47 b), 5-cyclopropyl-6-(1,1,1-trifluoropropan-2-yloxy)picolinic acid was reacted with 2-methyl-2-(methylamino)propan-1-ol (CAN 27646-80-6) in the presence of TBTU and DIEA to obtain the title compound as white solid; MS (EI): m/e=345.4 [MH+].