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HRID624884

反应详情

EQUATION

反应方程式

HRID 624884 的结构方程式

REACTANTS

反应物

4
结构：CC1(C)COCN1
HCID62010

4,4-Dimethyl oxazolidine

C5H11NO

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：CC(C)CS(=O)(=O)c1nc(C(=O)O)ccc1C1CC1
HCID71087731

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CS(=O)(=O)c1nc(C(=O)N2COCC2(C)C)ccc1C1CC1
HCID76282133

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in Example 47 b), 5-cyclopropyl-6-(isobutylsulfonyl)picolinic acid (Example 6 d)) was reacted with 4,4-dimethyloxazolidine (CAN 51200-87-4) in the presence of TBTU and DIEA to obtain the title compound as colorless solid; MS (EI): m/e=367.4 [MH+].