HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 90204312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 5-(chloromethyl)-1-methyl-1H-1,2,3,4-tetrazole | HCID 12205086 | — |
| Product | HCID 90204312 | HCID 90204312 | 72.2% |
Reaction Steps
A mixture of 2-methylpropan-2-amine (75-64-9, 281 mg, 404 μL, 3.85 mmol) and 5-(chloromethyl)-1-methyl-1H-tetrazole (57235-84-4, 100 mg, 754 μmol) was stirred at ambient temperature for 16 h and concentrated in vacuo to give the title compound (112 mg, 72%) as yellow solid; MS (EI): m/e=169 [M+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303012B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-953a4c53dda6492f89b1f02d723d08b5 |
| Source note | uspto-grants-2016_04 |