Tert-Butylamine → HCID 90204312, compound

HRID 624902Notes

Reaction equation

HRID 624902 reaction equation
[CH3:1][C:2]([NH2:5])([CH3:4])[CH3:3].[Cl:6][CH2:7][C:8]1[N:12]([CH3:13])[N:11]=[N:10][N:9]=1>>[ClH:6].[CH3:1][C:2]([NH:5][CH2:7][C:8]1[N:12]([CH3:13])[N:11]=[N:10][N:9]=1)([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 6385Tert-ButylamineHCID 122050865-(chloromethyl)-1-methyl-1H-1,2,3,4-tetrazole

Product 1

HCID 90204312HCID 90204312, compoundYield 72.2%

Procedure

A mixture of 2-methylpropan-2-amine (75-64-9, 281 mg, 404 μL, 3.85 mmol) and 5-(chloromethyl)-1-methyl-1H-tetrazole (57235-84-4, 100 mg, 754 μmol) was stirred at ambient temperature for 16 h and concentrated in vacuo to give the title compound (112 mg, 72%) as yellow solid; MS (EI): m/e=169 [M+].

Workup

  1. concentrationconcentrated in vacuo

Sources & evidence

ORD record
ord-953a4c53dda6492f89b1f02d723d08b5
Source dataset
uspto-grants-2016_04
Patent number
US09303012B2

Reaction notes

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