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HRID624906

反应详情

EQUATION

反应方程式

HRID 624906 的结构方程式

REACTANTS

反应物

4
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CC1(C)CCNCC1
HCID138100

Piperidine, 4,4-dimethyl-

C7H15N

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：O=C(O)c1ccc(C2CC2)c(OCC2CCCO2)n1
HCID71087254

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CCN(C(=O)c2ccc(C3CC3)c(OCC3CCCO3)n2)CC1
HCID76282136

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in Example 47 b), 5-cyclopropyl-6-(tetrahydro-furan-2-ylmethoxy)-pyridine-2-carboxylic acid (Example 4 b)) was reacted with 4,4-dimethyl-piperidine (4045-30-1) in the presence of TBTU and DIEA to obtain the title compound as colorless oil; MS (EI): m/e=359.6 [MH+].