HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid → HCID 76280803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid | HCID 71087346 | — |
| Reactant | HCID 90203546 | HCID 90203546 | — |
| Product | HCID 76280803 | HCID 76280803 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 47 b, using 5-cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid (Example 3 c, 100 mg, 429 μmol) and 4,4-dimethyl-pyrrolidine-2-carboxylic acid amide hydrochloride (84.3 mg, 472 μmol) as starting materials and isolated (145 mg, 95%) as white foam; LC-MS (UV peak area, ESI) 100%, 358.2124 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303012B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-43e3b11020374179bb8689e298bc2162 |
| Source note | uspto-grants-2016_04 |