HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 90203590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66630658 | HCID 66630658 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90203590 | HCID 90203590 | — |
Reaction Steps
In analogy to the procedure described in Example 82 a), (S)-tert-butyl 5-carbamoyl-2,2-dimethylpyrrolidine-1-carboxylate (CAN 1292838-05-1) was treated with a 4 M solution of HCl in dioxane to give the title compound as colorless solid which was sufficiently pure to be used in the next step; MS (EI): m/e=143.2 [(M-Cl)H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303012B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-3dbf7fd3a93e471292f22a33c97388dc |
| Source note | uspto-grants-2016_04 |