Hydrogen Bromide → HCID 89656205, compound

Participants

Reaction Steps

To a solution of (6-(3-(dimethylamino)propyl)pyridin-3-yl)(4-methoxy-phenyl)methanone (298 mg, 1 mmol) in 10 mL of methanol was added 10 mL of 48% HBr at rt and the mixture was heated to reflux for 3 h and cooled. The solvent was evaporated to give the crude product, which was used without further purification (284 mg, 100% yield).

Provenance & Evidence