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HRID626160

反应详情

EQUATION

反应方程式

HRID 626160 的结构方程式

REACTANTS

反应物

2
结构：CCC(=O)c1ccccc1
HCID7148

1-Phenylpropan-1-one

C9H10O

结构：CN(CCOc1ccc(C(=O)c2ccc(O)cn2)cc1)C(=O)OC(C)(C)C
HCID89656144

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=C(c1ccc(OCCNC)cc1)c1ccc(O)cn1)c1ccccc1
HCID78135504

未命名化合物

PROCEDURE

实验过程

Following general procedure of McMurry reaction as described in example 1, step B, tert-butyl 2-(4-(5-hydroxypicolinoyl)phenoxy)ethyl(methyl)carbamate (1.0 eq) was reacted with propiophenone (3.0 eq) to give the desired product (Z/E=1/1). m/z=375[M+1]+.

WORKUP

后处理

  1. customgeneral procedure of McMurry reaction