HRID626195

反应详情

EQUATION

反应方程式

HRID 626195 的结构方程式

PROCEDURE

实验过程

Following general procedure of McMurry reaction as described in example 1, step B, 1-(6-hydroxypyridin-3-yl)propan-1-one (0.3 g, 1.0 eq) was reacted with (4-(2-chloroethoxy)phenyl)(4-hydroxyphenyl)methanone (1.37 g, 2.5 eq) to give the desired Z-product (Z and E isomer can be separated via column chromatography).

WORKUP

后处理

  1. customgeneral procedure of McMurry reaction
  2. customto give the desired
  3. customZ-product (Z and E isomer can be separated via column chromatography)