Lithium hydroxide, monohydrate → HCID 72195494, compound

HRID 626334Notes

Reaction equation

HRID 626334 reaction equation
C([O:3][C:4](=[O:32])[CH2:5][O:6][C:7]1[CH:12]=[CH:11][CH:10]=[C:9]([NH:13][C:14]([C:16]2[C:25]3[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=3)[CH:19]=[C:18]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[CH:17]=2)=[O:15])[CH:8]=1)C.O[Li].O>>[C:26]1([C:18]2[CH:17]=[C:16]([C:14]([NH:13][C:9]3[CH:8]=[C:7]([CH:12]=[CH:11][CH:10]=3)[O:6][CH2:5][C:4]([OH:32])=[O:3])=[O:15])[C:25]3[C:20]([CH:19]=2)=[CH:21][CH:22]=[CH:23][CH:24]=3)[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=1

Participants

3

Procedure

Compound 9a was synthesized from 8a (0.21 mmol) and LiOH.H2O (0.63 mmol) using the procedure according to the above Method E.

Sources & evidence

ORD record
ord-7ac3c110217d44d6a63d7b3c243e0f77
Source dataset
uspto-grants-2016_04
Patent number
US09309187B2

Reaction notes

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