Lithium hydroxide, monohydrate → HCID 72195496, compound

HRID 626335Notes

Reaction equation

HRID 626335 reaction equation
C([O:3][C:4](=[O:33])[CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([Cl:13])=[C:9]([NH:14][C:15]([C:17]2[C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH:20]=[C:19]([C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=3)[CH:18]=2)=[O:16])[CH:8]=1)C.O[Li].O>>[Cl:13][C:10]1[CH:11]=[CH:12][C:7]([O:6][CH2:5][C:4]([OH:33])=[O:3])=[CH:8][C:9]=1[NH:14][C:15]([C:17]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[CH:20]=[C:19]([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[CH:18]=1)=[O:16]

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 131735214HCID 131735214, compound

Product 1

HCID 72195496HCID 72195496, compound

Procedure

Compound 9c was synthesized from 8c (0.23 mmol) and LiOH.H2O (0.71 mmol) using the procedure according to the Method E described above.

Sources & evidence

ORD record
ord-4eafad5ce99d4267a3531df397b3fe0a
Source dataset
uspto-grants-2016_04
Patent number
US09309187B2

Reaction notes

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