Lithium hydroxide, monohydrate → HCID 72195629, compound

HRID 626336Notes

Reaction equation

HRID 626336 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5](/[CH:8]=[CH:9]/[C:10]([O:12]CC)=[O:11])=[CH:4][C:3]=1[NH:15][C:16]([C:18]1[C:27]2[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:21]=[C:20]([C:28]2[CH:33]=[CH:32][CH:31]=[C:30]([F:34])[CH:29]=2)[CH:19]=1)=[O:17].O[Li].O>>[F:34][C:30]1[CH:29]=[C:28]([C:20]2[CH:19]=[C:18]([C:16]([NH:15][C:3]3[CH:4]=[C:5](/[CH:8]=[CH:9]/[C:10]([OH:12])=[O:11])[CH:6]=[CH:7][C:2]=3[F:1])=[O:17])[C:27]3[C:22]([CH:21]=2)=[CH:23][CH:24]=[CH:25][CH:26]=3)[CH:33]=[CH:32][CH:31]=1

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 90057965HCID 90057965, compound

Product 1

HCID 72195629HCID 72195629, compound

Procedure

Compound 17b was synthesized from 16b (0.5 mmol) and LiOH.H2O (5 mmol) using the procedure according to the Method E described above.

Sources & evidence

ORD record
ord-39b6317349ab4bb38ee1ef9738329141
Source dataset
uspto-grants-2016_04
Patent number
US09309187B2

Reaction notes

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