Lithium hydroxide, monohydrate → HCID 72195764, compound

HRID 626341Notes

Reaction equation

HRID 626341 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5](/[CH:8]=[CH:9]/[C:10]([O:12]CC)=[O:11])=[CH:4][C:3]=1[NH:15][C:16]([C:18]1[C:27]2[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:21]=[C:20]([C:28]2[CH:33]=[C:32]([OH:34])[CH:31]=[C:30]([F:35])[CH:29]=2)[CH:19]=1)=[O:17].O[Li].O>>[F:1][C:2]1[CH:7]=[CH:6][C:5](/[CH:8]=[CH:9]/[C:10]([OH:12])=[O:11])=[CH:4][C:3]=1[NH:15][C:16]([C:18]1[C:27]2[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:21]=[C:20]([C:28]2[CH:33]=[C:32]([OH:34])[CH:31]=[C:30]([F:35])[CH:29]=2)[CH:19]=1)=[O:17]

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 117951711HCID 117951711, compound

Product 1

HCID 72195764HCID 72195764, compound

Procedure

Compound 17g was synthesized from 16g (0.42 mmol) and LiOH.H2O (4.2 mmol) using the procedure according to Method E described above.

Sources & evidence

ORD record
ord-e348bdc2b8884732989ca65fe1044b09
Source dataset
uspto-grants-2016_04
Patent number
US09309187B2

Reaction notes

Loading…