Lithium hydroxide, monohydrate → HCID 72195768, compound

HRID 626345Notes

Reaction equation

HRID 626345 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:9]=[C:10]([C:18]([NH:20][C:21]3[CH:22]=[C:23](/[CH:27]=[CH:28]/[C:29]([O:31]CC)=[O:30])[CH:24]=[CH:25][CH:26]=3)=[O:19])[C:11]3[C:16]([CH:17]=2)=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:5]=[CH:6][CH:7]=1.O[Li].O>>[OH:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:9]=[C:10]([C:18]([NH:20][C:21]3[CH:22]=[C:23](/[CH:27]=[CH:28]/[C:29]([OH:31])=[O:30])[CH:24]=[CH:25][CH:26]=3)=[O:19])[C:11]3[C:16]([CH:17]=2)=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 117951670HCID 117951670, compound

Product 1

HCID 72195768HCID 72195768, compoundYield 44%

Procedure

Compound 25a was synthesized from 24a (1.02 mmol) and LiOH.H2O (10.3 mmol) using procedure according to the Method E described above.

Sources & evidence

ORD record
ord-a265f810bbd349a495dda342fe23614e
Source dataset
uspto-grants-2016_04
Patent number
US09309187B2

Reaction notes

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