HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-N-((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide → (S)-1-(3-isopropylphenyl)ethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-N-((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide | HCID 86732637 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (S)-1-(3-isopropylphenyl)ethanamine | HCID 86674570 | — |
Reaction Steps
The mixture of (S)—N—((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide (6.1 g, 0.023 mol) in methanol was stirred at room temperature for 3 hours and then concentrated and evaporated with toluene for three times to give the titled compound which was without purification for next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309227B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-6aa35cfe6d984e308516c2debcf98c03 |
| Source note | uspto-grants-2016_04 |