HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(4-Bromophenyl)ethylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86732639 | HCID 86732639 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(4-Bromophenyl)ethylamine hydrochloride | HCID 53484870 | — |
Reaction Steps
(S)—N—((S)-1-(4-bromophenyl)ethyl)-2-methylpropane-2-sulfinamide (170 mg, 0.56 mmol) was dissolved in methanol (2 mL) followed by addition of con.HCl (1 mL). The mixture was stirred at RT for 4 h and then was concentrated and evaporated with toluene twice to afford the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309227B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-2c4a12918ec54afba31feacce594bbd3 |
| Source note | uspto-grants-2016_04 |