Benzonitrile, 2-amino-3-chloro-5-nitro- → HCID 178510232, compound

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Reaction Steps

Following the procedure described for [1-(4-azido-5-fluoropyridin-3-yl)-meth-(E)-ylidene]-(2,6-dichloro-4-nitrophenyl)-amine (Example 99, Step 1), 2-amino-3-chloro-5-nitrobenzonitrile was stirred at room temperature to afford the title compound which was used without purification (6.07 g, quantitative yield). LCMS (Method C): RT=3.69 min, m/z: 318 [M+H+−N2].

Provenance & Evidence