HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropyl methyl ketone → N-[(E)-1-cyclopropylethylideneamino]-2,4,6-tri(propan-2-yl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropyl methyl ketone | HCID 13004 | — |
| Reactant | N-[(E)-3-methylbutan-2-ylideneamino]-2,4,6-tri(propan-2-yl)benzenesulfonamide | HCID 12563993 | — |
| Product | N-[(E)-1-cyclopropylethylideneamino]-2,4,6-tri(propan-2-yl)benzenesulfonamide | HCID 12735383 | — |
Reaction Steps
The title compound was prepared from 2,4,6-triisopropylbenzenesulfonyl hydrazide (Aldrich, 20 g, 67.01 mmol) and 1-cyclopropylethanone (Aldrich, 6.28 mL, 67.01 mmol) following the procedure described for Intermediate 33. The desired product was obtained as a white solid (15 g, 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309245B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-8a4383744e7747509882559eaa8dabe1 |
| Source note | uspto-grants-2016_04 |