反应详情

温度

80 °C

In a 100-mL round-bottom flask was placed a solution of 6-fluoropyridine-3-carboxylic acid (5.0 g, 35.4 mmol) in thionyl chloride (20 mL). The resulting solution was heated at 80° C. for 2 hours and concentrated under vacuum to give the title compound as a yellow oil.

1. customIn a 100-mL round-bottom flask was placed
2. concentrationconcentrated under vacuum