HRID6275

反应详情

EQUATION

反应方程式

HRID 6275 的结构方程式

PROCEDURE

实验过程

Trichlorosilane and allyl chloride were subjected to hydrosilylation reaction in a solvent in the presence of a platinum catalyst, followed by esterification reaction with methanol and urea and further by distillation to obtain γ-chloropropyltrimethoxysilane. The thus obtained γ-chloropropyltrimethoxysilane and potassium acrylate were subjected to desalting in a solvent, followed by removal of potassium chloride. Subsequently, low boiling components including the solvent were distilled off under reduced pressure to obtain crude γ-acryloxypropyltrimethoxysilane having a purity of approximately 90%.

WORKUP

后处理

  1. customfollowed by removal of potassium chloride
  2. distillationwere distilled off under reduced pressure