HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-Pentenoic Acid → Methyl 2-aminopent-4-enoate--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-Pentenoic Acid | HCID 14044 | — |
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Product | Methyl 2-aminopent-4-enoate--hydrogen chloride (1/1) | HCID 11332668 | 79.2% |
Reaction Steps
A solution of α-Allyl-Gly-OH (1.00 g, 7.75 mmol) in MeOH/HCl (20 mL) was heated at reflux for 3 hrs. After TLC showed the reaction was complete, the mixture was evaporated to give α-Allyl-Gly-OMe HCl (1.10 g, 79.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309285B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-ba820e9d904241959d30634df0f569b1 |
| Source note | uspto-grants-2016_04 |