HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 131735323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | N-Boc-O-allyl-L-homoserine | HCID 58798660 | — |
| Product | HCID 131735323 | HCID 131735323 | 98.9% |
Reaction Steps
A solution of Boc-L-HomoSer(O-allyl)-OH (4.50 g, 17.4 mmol) in HCl/MeOH (50 mL) was stirred at 20° C. for 6 hrs. The solvent was removed at reduced pressure to give Boc-L-HomoSer(allyl)-OMe HCl (3.60 g, 98.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309285B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-26416241fef946b4853cd7d92f9d5d07 |
| Source note | uspto-grants-2016_04 |