HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-difluoro-N-methylaniline → N-(2,4-difluorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-difluoro-N-methylaniline | HCID 2737023 | — |
| Reactant | 4,5-Dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxylic acid | HCID 56834053 | — |
| Product | N-(2,4-difluorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide | HCID 44242493 | — |
Reaction Steps
Following General Procedure C, 156 is prepared from 4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxylic acid and 2,4-difluoro-N-methylaniline. MS: (ESI+) 371.9
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309265B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-395df252b6904ca999742bf9a7e82966 |
| Source note | uspto-grants-2016_04 |