HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 3-(benzylamino)benzoate → HCID 3681313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 3-(benzylamino)benzoate | HCID 24973583 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 3681313 | HCID 3681313 | — |
Reaction Steps
A solution of 3-benzylamino-benzoic acid tert-butyl ester (1 g, 3 mmol) in trifluoroacetic acid/dichloromethane (1:5 v/v) (100 ml) was stirred for 16 hrs. The reaction was concentrated to dryness in vacuo to afford the title compound as a white solid. HPLC retention time 2.59 min. Mass spectrum (ES+) m/z 227.8 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447033B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-4bc2eb90970346a891c68c1f5cbee983 |
| Source note | uspto-grants-2016_09 |