HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hexafluoroantimonate → HCID 19734742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hexafluoroantimonate | HCID 16689647 | — |
| Reactant | Tris(p-methylbenzyl)sulfonium tetrafluoroborate | HCID 19795292 | — |
| Product | HCID 19734742 | HCID 19734742 | 87.3% |
Reaction Steps
Analogously to Example 4c), 100 g (230 mmol) of tris(p-methylbenzyl)sulfonium tetrafluoroborate are reacted with 119.0 g (460 mmol) of sodium hexafluoroantimonate. Recrystallization in isopropanol gives 117.1 g (87% of theory) of tris(p-methylbenzyl)sulfonium hexafluoroantimonate in the form of white crystals of melting point 88°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05247113 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-dcb6757025c842f682ae2753a298d10d |
| Source note | uspto-grants-1993_09 |