HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 4-butyl-3,5-dimethyl-1H-pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 3-Butylpentane-2,4-dione | HCID 73763 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-butyl-3,5-dimethyl-1H-pyrazole | HCID 12933276 | 102.6% |
Reaction Steps
At room temperature, to a mixture of 3-butyl-pentane-2,4-dione 7 g and ethanol 70 ml was added hydrazine one hydrate 3.3 g and the resulting mixture was stirred for twelve hours. The reaction mixture was subjected to a silica gel column chromatography to give 4-butyl-3,5-dimethyl-1H-pyrazole 7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09314023B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-b936d19030ab41229f494a98cfba8d5a |
| Source note | uspto-grants-2016_04 |