HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 628773Generated: October 29, 2026
Sodium Sulfite → Sodium 4-(methylsulfonyl)benzenesulfinate
https://huagongshe.com/reaction/628773
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 4-Methanesulfonylbenzene-1-sulfonyl chloride | HCID 2735182 | — |
| Solvent | Water | HCID 962 | — |
| Product | Sodium 4-(methylsulfonyl)benzenesulfinate | HCID 23674706 | — |
Reaction Steps
To a solution of 0.57 g of NaHCO3 (7.1 mmol) and 1.1 g of Na2SO3 (8.8 mmol) in water (5.0 mL) were added 1.0 g (3.9 mmol) of 4-methanesulfonyl-benzenesulfonyl chloride. The reaction was heated at 80° C. for 3 h. The solvent was removed under reduced pressure. The filtrate was concentrated under reduced pressure to give sodium 4-methanesulfonyl-benzenesulfinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09315454B2 |
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| Source dataset | uspto-grants-2016_04 |
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| ORD ID | ord-eee063b1ea7847d9bb15f851c405b8b5 |
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| Source note | uspto-grants-2016_04 |
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