HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(((1-Naphthylmethyl)thio)methyl)naphthalene → Bis(1-naphthylmethyl)ethylsulfonium hexafluoroantimonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(((1-Naphthylmethyl)thio)methyl)naphthalene | HCID 233907 | — |
| Reactant | Triethyloxonium hexafluoroantimonate | HCID 22239852 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Bis(1-naphthylmethyl)ethylsulfonium hexafluoroantimonate | HCID 19795277 | 98.5% |
Reaction Steps
5.0 g (15.9 mmol) of bis(1-naphthylmethyl) sulfide and 5.93 g (17.5 mmol) of triethyloxonium hexafluoroantimonate in 30 ml of methylene chloride are reacted according to Example 1a) to give 9.07 g (98% of theory) of bis(1-naphthylmethyl)ethylsulfonium hexafluoroantimonate in the form of white crystals of melting point 101°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05247113 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-b72b1df24dfd40c49dba15fa1f93e2ed |
| Source note | uspto-grants-1993_09 |