HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromothiophene-2-carbaldehyde → HCID 118228960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromothiophene-2-carbaldehyde | HCID 78428 | — |
| Reactant | But-3-en-1-ylboronic acid | HCID 20827003 | — |
| Product | HCID 118228960 | HCID 118228960 | 55% |
Reaction Steps
The compound was synthesized as in Example 3.1 using 5-bromo-2-formylthiophene (191 mg, 1.0 mmol) in place of 5-bromo-2-formylfuran and 3-butenylboronic acid (150 mg, 1.5 mmol) in place of hexylboronic acid to give 5-(3-butenyl)-2-formylthiophene (91 mg, 55%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-ed5a3e92483f4f2ea60c3a8f53eed495 |
| Source note | uspto-grants-2016_04 |