HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → 2-Methyl-4-[(propan-2-yl)oxy]benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 4-Hydroxy-2-methylbenzaldehyde | HCID 458185 | — |
| Product | 2-Methyl-4-[(propan-2-yl)oxy]benzaldehyde | HCID 13087978 | 76% |
Reaction Steps
The compound was synthesized as in Example 87.1, using 4-hydroxy-2-methylbenzaldehyde (54.4 mg, 0.40 mmol) in place of 4-hydroxybenzaldehyde and 2-iodopropane (100 μL, 0.80 mmol) in place of 1-iodo-(3,3,3-trifluoro)propane to give 2-methyl-4-isopropoxybenzaldehyde (54 mg, 76%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-a5a6120f75b04621a2d6eaa3f1d42723 |
| Source note | uspto-grants-2016_04 |