HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-2-methylbenzaldehyde → HCID 82005921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-2-methylbenzaldehyde | HCID 458185 | — |
| Reactant | 1,1-Difluoro-2-iodoethane | HCID 3833565 | — |
| Product | HCID 82005921 | HCID 82005921 | 68% |
Reaction Steps
The compound was synthesized as in Example 87.1, using 4-hydroxy-2-methylbenzaldehyde (54.4 mg, 0.40 mmol) in place of 4-hydroxybenzaldehyde and 2,2-difluoro-1-iodoethane (153 mg, 0.80 mmol) in place of 1-iodo-(3,3,3-trifluoro)propane to give 4-(2,2-difluoroethoxy)-2-methylbenzaldehyde (54 mg, 68%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-bfe1137986d6430ab6b9f7081bb9d923 |
| Source note | uspto-grants-2016_04 |