HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)pyridine hydrobromide → HCID 178429435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)pyridine hydrobromide | HCID 2734720 | — |
| Reactant | HCID 178429541 | HCID 178429541 | — |
| Product | HCID 178429435 | HCID 178429435 | 86% |
Reaction Steps
As per procedure from Example 1, 2-(bromomethyl)pyridine hydrobromide and 6-methyl-2-sulfanylpyrimidin-4-ol were combined to provide the title compound as a white solid (86% yield); 1H NMR (400 MHz, DMSO-d6): δ 2.68 (s, 3H), 4.47 (s, 2H), 6.00 (s, 1H), 7.25 (dd, 1H), 7.47 (d, 1H), 7.72 (dd, 1H), 8.50 (d, 1H); M+234.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315521B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-943a3fcf0c6342ed9c98c4973e0e1ee1 |
| Source note | uspto-grants-2016_04 |