HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methoxyphenylboronic acid → HCID 118666086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methoxyphenylboronic acid | HCID 4157211 | — |
| Reactant | HCID 118666104 | HCID 118666104 | — |
| Product | HCID 118666086 | HCID 118666086 | — |
Reaction Steps
Suzuki reaction of 1-(5-bromopyrimidin-2-yl)-N,N-dimethyl-3-(methylsulfinyl)-1H-indole-6-carboxamide (0.15 g, 0.37 mmol; intermediate in the preparation of synthesis example 267) with 2-fluoro-5-methoxyphenylboronic acid (0.13 g, 0.74 mmol) in analogy to the procedure detailed for example 261). White solid. Yield: 0.06 g (36% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315490B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-554818f2433c4f8490c37d743daa5bc3 |
| Source note | uspto-grants-2016_04 |