Ethylenediamine → HCID 89825998, compound

Participants

Reaction Steps

To 2-bromo-6-fluoro-4-methyl-pyridine (380 mg, 2 mmol) was added potassium carbonate (552 mg, 4 mmol) followed by ethylenediamine (3 ml) and the resulting mixture was stirred art room temperature for two hours. The mixture was filtered through kieselguhr and the filtrate was evaporated to dryness under reduced pressure to yield 256 mg (1.11 mmol, 56%) MS(ESI) m/z=230.0 [M+1]+.

Provenance & Evidence