Ethylenediamine → HCID 89825830, compound

Participants

Reaction Conditions

Reaction Steps

3-Chloro-5-cyclopropyl-1,2,4-oxadiazol (72 mg, 0.5 mmol) and TEA (139 μl, 1 mmol) were dissolved in ethane-1,2-diamine (3 ml), placed in a sealed tube and heated at 125° C. for 2 hours. The mixture was cooled to room temperature and evaporated to dryness under reduced pressure and used directly in the next step MS(ESI) m/z=169.1 [M+1]+.

Provenance & Evidence