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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 631881Generated: October 30, 2026

HCID 68296408, compound → HCID 68296409, compound

https://huagongshe.com/reaction/631881

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68296408HCID 68296408—
ReactantHCID 178418361HCID 178418361—
CatalystPlatinumHCID 23939—
SolventEthanolHCID 702—
ProductHCID 68296409HCID 6829640994.8%

Reaction Steps

1-Benzyl-5-(2-methoxy-6-nitrophenyl)-1H-tetrazole (Intermediate 14, 0.14 g) was dissolved in ethanol (5 mL) under a nitrogen atmosphere. Platinum on carbon (10%, 0.01 g) was added and the nitrogen atmosphere was replaced by hydrogen. The mixture was stirred for 18 hours and then filtered through celite. The filtrate was evaporated to dryness to give the title compound as a brown gum (0.12 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09321740B2
Source datasetuspto-grants-2016_04
ORD IDord-31c0d21fadf54400adfb63c136180632
Source noteuspto-grants-2016_04