HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68296408, compound → HCID 68296409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68296408 | HCID 68296408 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68296409 | HCID 68296409 | 94.8% |
Reaction Steps
1-Benzyl-5-(2-methoxy-6-nitrophenyl)-1H-tetrazole (Intermediate 14, 0.14 g) was dissolved in ethanol (5 mL) under a nitrogen atmosphere. Platinum on carbon (10%, 0.01 g) was added and the nitrogen atmosphere was replaced by hydrogen. The mixture was stirred for 18 hours and then filtered through celite. The filtrate was evaporated to dryness to give the title compound as a brown gum (0.12 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321740B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-31c0d21fadf54400adfb63c136180632 |
| Source note | uspto-grants-2016_04 |