HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-6-(3-chloro-phenyl)-pyridine-2-carboxylic acid → 5-Chloro-6-(3-chloro-phenyl)-pyridine-2-carboxylic acid (1-methyl-1-oxazol-2-yl-ethyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-6-(3-chloro-phenyl)-pyridine-2-carboxylic acid | HCID 71087619 | — |
| Reactant | alpha,alpha-Dimethyl-2-oxazolemethanamine | HCID 82418817 | — |
| Product | 5-Chloro-6-(3-chloro-phenyl)-pyridine-2-carboxylic acid (1-methyl-1-oxazol-2-yl-ethyl)-amide | HCID 71105594 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 1, using 5-chloro-6-(3-chloro-phenyl)-pyridine-2-carboxylic acid (Example 58 c) and α,α-dimethyl-2-oxazolemethanamine (CAN 1211519-76-4) as starting materials, MS (EI): m/e=376.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321727B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-88f9a73943914862968b817cfb3338b9 |
| Source note | uspto-grants-2016_04 |