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HRID632359

反应详情

EQUATION

反应方程式

HRID 632359 的结构方程式

REACTANTS

反应物

3
结构：CNC(=O)[C@@H](N)CC(C)(C)C
HCID57635521

未命名化合物

结构：O=C(O)c1cccc(OCC(F)(F)C(F)(F)F)n1
HCID86674786

未命名化合物

结构：O=C(O)c1ccc(C2CC2)c(OCC(F)(F)C(F)(F)F)n1
HCID86674787

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)[C@H](CC(C)(C)C)NC(=O)c1ccc(C2CC2)c(OCC(F)(F)C(F)(F)F)n1
HCID86674789

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 1, using the mixture of 6-(2,2,3,3,3-pentafluoro-propoxy)-pyridine-2-carboxylic acid and 5-cyclopropyl-6-(2,2,3,3,3-pentafluoro-propoxy)-pyridine-2-carboxylic acid (Example 297b) and (2S)-2-amino-N,4,4-trimethyl-pentanamide (CAN 1160161-70-5) as starting materials, the product was isolated by preparative HPLC; LC-MS (UV peak area/ESI) 100%, 452.1962 (M+H)+.

WORKUP

后处理

  1. customthe product was isolated by preparative HPLC