HRID632518

反应详情

EQUATION

反应方程式

HRID 632518 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To 0.72 g of [2-methyl-4-(2-pyridylmethoxy)phenyl]methanol were added 30 mL of CHCl3 and 7.2 g of manganese dioxide, and the mixture was stirred at room temperature for 2 hours. Insoluble matter was filtered off from the reaction mixture, and the mother liquor was concentrated to give 0.70 g of the title compound (99% yield).

WORKUP

后处理

  1. filtrationInsoluble matter was filtered off from the reaction mixture
  2. concentrationthe mother liquor was concentrated