HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2-Methyl-4-(2-pyridylmethoxy)phenyl]methanol → 2-Methyl-4-(2-pyridylmethoxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2-Methyl-4-(2-pyridylmethoxy)phenyl]methanol | HCID 117888981 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Methyl-4-(2-pyridylmethoxy)benzaldehyde | HCID 117888978 | 99% |
Reaction Steps
To 0.72 g of [2-methyl-4-(2-pyridylmethoxy)phenyl]methanol were added 30 mL of CHCl3 and 7.2 g of manganese dioxide, and the mixture was stirred at room temperature for 2 hours. Insoluble matter was filtered off from the reaction mixture, and the mother liquor was concentrated to give 0.70 g of the title compound (99% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321752B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-66b6ed5d60fd4d7abd68002c09eb2c15 |
| Source note | uspto-grants-2016_04 |