huagongshe.com
HRID633068

反应详情

EQUATION

反应方程式

HRID 633068 的结构方程式

REACTANTS

反应物

3
结构：CCS(=O)(=O)Cl
HCID11667

Ethanesulfonyl chloride

C2H5ClO2S

结构：CC(C)S(=O)(=O)Cl
HCID82408

Isopropyl sulfonyl chloride

C3H7ClO2S

结构：CCS(=O)(=O)Cc1ccc(C(=O)Nc2ccc(Cl)c(-c3ccccn3)c2)cc1
HCID58614777

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)S(=O)(=O)Cc1ccc(C(=O)Nc2ccc(Cl)c(-c3ccccn3)c2)cc1
HCID58614855

未命名化合物

PROCEDURE

实验过程

N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(isopropylsulfonylmethyl)benzamide was prepared using the same procedure as N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(ethylsulfonylmethyl)benzamide except propane-2-sulfonyl chloride was substituted for ethanesulfonyl chloride. The product was purified on reverse phase HPLC to yield N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(isopropylsulfonylmethyl)benzamide. MS (Q1) 429 (M)+.

WORKUP

后处理

  1. customN-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(isopropylsulfonylmethyl)benzamide was prepared
  2. customThe product was purified on reverse phase HPLC